Would someone mind proofreading this,
Im writing a formal lab report on an experiment of gravimetric analysis, I am writing my abstract and am stuck at these last two sentences. "The purpose of experiment 4 was to determine the chloride content of an unknown soluble chloride sample using gravimetric analysis. Gravimetric analysis is a technique that is based on the quantitative isolation of a desired constituent. This form of analysis involves comparing the masses of two compounds in order to determine the amount of constituent present in an unknown sample."
Gravimetric analysis is a technique that is based on the quantitative determination of the mass of an analyte. Maybe I would change it to this, what you have seems pretty accurate. The last sentence could also potentially be changed from constituent to compound/element or analyte
Actually you should be fine using constituent.
It is important to mention mass when you explain gravimetric analysis because it really is just the determination of mass of a compound in a sample
oh thats great! that sentence sounds much better actually. :) So would you recommend that i leave the last sentence as is?
Tbh I don't really like the last sentence but it is alright maybe change constituent to analyte
doesn't matter though actually
it is fine, I dont see why a teacher/prof would deduct marks for that
or TA
haha, well thank you i appreciate your honesty and help! :) Ill see what i do with it. Starting off is always the most difficult part after i can go back and proofread
Well an abstract you should always write last
if you are doing an abstract I assume you are doing an introduction though
sorry I'm pretty sleep deprived
touche. I am all done with the rest, just have this left!
don't worry about it at least your honest!
What technique did you perform out of interest?
We used gravimetric analysis using vacuum filtration ;p
Oh so you just did a precipitation, then vacuum filtered, put it in a desiccator, then weigh it. Then just use gravimetric factor and a balanced reaction equation to get back to the original amount of compound present in your sample
how are you comparing the masses of two compounds?
I'm making assumptions though I dont really know what you did in your experiment
yes exactly that! Well to be honest chemistry is not my best subject so for the most part i just wing it :/
So you just used the balanced equation to figure out the original amount of compound present in your solution. So how did you use two masses?
you should really only need to use the mass of precipitate to find the mass of the original compound
If you are referring to gravimetric factor then yeah you use two molecular masses
no we didn't use a balanced equation. basically we found the mass of AgCl used and from there used that mass to determine the amount of Cl in the original sample. & from thereee we calculated the percent of Cl in the unknown sample
So you did a titration
kind of
Sort of. I do have a question though if you mind helping
No problem ask away
At the end of the lab our professor has us calculate an average percent among myself and another two students. What is the purpose of doing that?
What does the average percent show? or tell you? was very confused
Can you show me the formula?
Oh wait one sec
ill show you my calculations but it was basically finding the mean percent
Well when you do an experiment you should always do it at least in triplicate as this gets you close to the real value
so when you take an average percentage you are getting closer to the real percentage
at least I'm speaking in an experimental sense
in terms of that example you gave me it is more of an indicator how a group of people did on an exam, although mean has a problem in that extreme values can throw it off
So just say, a three people get a 10%, 50% and 51% So the average is 37%, which I would say is pretty miss representative of the actual values (although this example is not very good, because of the small amount of values, it is like taking the average of a large group of middle class peoples net worth and then also including bill gates net worth, the value you get is going to be way off). I'm going on a tangent though
This is something you should be a aware of as if you get outliers in your experiments you should tell your prof/teacher about it and see if it is possible to ignore
ok I'm done rambling about percentages do you kind of follow?
yes i understand it better. However, in my case all the percents we close to the average value so would that mean the average is a good representation of the data
Well there is precision and accuracy
A high precision is when the values are very close together in this case the precentages, the accuracy you have no idea unless you have a reference to compare to
wellll
I think you used a standard though in your experiment
For my given sample i was given the theoretical value
It would mean you have good precision I think
i calculated the percent of Cl in the unknown sample to be 57.29% & the theoretical value was 57.59 %
precision is hitting the same spot on the dart board, accuracy is hitting the center of the dart board
Where are you getting the theoretical value? Sorry not really sure I completely understand what you did in your experiment not that you need to explain it
hah its ok! Well each student was given an unknown sample #, mine was #53. Once i finished my experiment i calculated the Cl mass in the unknown and the percent of Cl in the sample. In addition my professor gave us each our theoretical values based on which sample number we got
kinda make sense?
Yes it makes loads of sense
You can say that your experiment was successful in identifying the amount of analyte present in the sample relative to the theoretical within (Theoretical % - experimental %)
or something like that
You could say it is close but when you write scientific literature you want to avoid being subjective
When ever comparing two things you need a reference
but again I'm rambling blah
Does that kind of help?
no i totally understand! much better
You can try to rationalize opinions though
one more thing!
If you have other data to show that it is not really an opinion, and more a logical conclusion
If you dont follow that last part dont worry about it.
when you said, "the amount of analyte present in the sample relative to the theoretical within (Theoretical % - experimental %) ". In the parenthesis would that value just be the difference among the two?
ask away I need to go soon need to finish my food and study
yeah you would just show how close the theoretical value is from the experimental, you could also use percent yield which just shows how close the experimental is to the theoretical yield, but that is more used for synthesis problems
from that the reader could say oh that is close or oh that is far away I dont know
oh sorry synthesis experiments
ahh ok. i understand i think I'm good now :) Thank you so much!
No problem good luck in chemistry and your lab report :)
and on*
thank you so much! :)
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